- Created by Wirth, Justin C, last modified on May 06, 2024
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2024-12-20 to 2025-01-02: Reduced Holiday Operations
Dear Birck Research Community,
The Purdue winter recess begins effective Friday afternoon December 20th and concludes Thursday morning, January 2. The university is officially closed during this time. As we have done in past years, the Birck Nanotechnology Center will remain available for research but will be unstaffed and hazardous gasses will be unavailable. Lab work may otherwise proceed, though any fume hood work must be done with someone else present in the same laboratory or cleanroom bay (the "buddy" system). Click the link above to get more detail about equipment conditions and rules.
Refer to the Material and Process Compatibility page for information on materials compatible with this tool.
Equipment Status: Set as UP, PROBLEM, or DOWN, and report the issue date (MM/DD) and a brief description. Italicized fields will be filled in by BNC Staff in response to issues. See Problem Reporting Guide for more info.
Status | DOWN |
Issue Date and Description | Extended electrical shutdown necessary for JEOL 2 install |
Estimated Fix Date and Comment | System should be available and calibrated by 5 PM. |
Responding Staff |
iLab Name | |
---|---|
iLab Kiosk | |
FIC | Shared |
Owner | |
Location | BRK 2100P |
Max. Wafer | 6"/150 mm |
Info Links | SOP | /wiki/spaces/BNCWiki/pages/6232822 | /wiki/spaces/BNCWiki/pages/6232164 |
Overview
General Description
The new JEOL JBX-8100FS series spot beam lithography system is designed for higher throughput and lower operating costs. The JBX-8100FS writes ultrafine patterns at a faster rate of speed while minimizing idle time, especially during the exposure process, thus increasing throughput. This new, high precision compact e-beam tool is suitable for a wide range of applications from research to production, while its small footprint and low power consumption reduce cost of ownership.
Main Features
Small footprint
The area required for the standard system is 4.9 m (W) x 3.7 m (D) x 2.6 m (H), much smaller than the conventional systems.Low power consumption
Power needed for normal operation is approximately 3 kVA, reduced to 1/3 of the conventional systems.High throughput
The system has two exposure modes, high resolution and high throughput modes, supporting different types of patterning from ultra fine processing to small to mid size production. It has minimized the idle time during exposure while increasing the maximum scanning speed by 1.25 to 2.5 times to 125 MHz (the world’s highest level) for high speed writing.Version
The JBX-8100FS is available in 2 versions: G1 (entry model) and G2 (full option model). Optional accessories can be added to the G1 model as needed.New Functions
An optional optical microscope is available to enable examination of patterns on the sample without exposing resist to light. A signal tower is provided as standard for visual monitoring of system operation.Laser positioning resolution
Stage positions are measured and controlled in 0.6 nm steps as standard, and in 0.15 nm steps with an optional upgrade.System control
Versatile Linux® operating system combined with a new graphic user interface provides ease in operation. The data preparation program supports both Linux® and Windows®.
Specifications
The JBX-8100FS is an electron-beam lithography system designed to write nanometer to submicron sized patterns using a spot beam.
Write Modes Specifications
Note: High Throughput will be almost exclusively used, contact Bill Rowe if you think you need HR mode.
High Throughput | High Resolution | |
Max. Main Field Size | 1000 μm x 1000 μm | 100 μm x 100 μm |
Max. Sub Field Size | 8 μm x 8 μm | 0.8 μm x 0.8 μm |
Min. Beam Step Size | 0.5 nm | 0.05 nm |
Min. Shape Placement Step | 1 nm | 0.1 nm |
Overlay Accuracy | ≤±20 nm | ≤±9 nm |
Field Stitching Accuracy | ≤±20 nm | ≤±9 nm |
Min. Beam Diameter | 5.1 nm | 1.8 nm |
Min. Line Width (Field Center) | <12 nm | <8 nm |
Available Currents (at BNC) | 2, 10, 30, 100 nA (200 nA available as a test file) | 0.5 nA |
Features
ZrO/W emitter
4-stage electron-beam focusing system
Accelerating voltage: 100 kV
Writing: Vector scan (within a subfield) and Step-and-repeat (electronically between subfields and physically between fields).
Beam scanning speed: ≤125 MHz
Scan speed modulation: 256 rank / 0.05 nsec resolution
Mainfield/Positioning DAC: 20-bit
Subfield/Scanning DAC: 14-bit
Focus range: ±100 μm
Max wafer size: 200 mm
Max writing area: 150 mm x 150 mm
Movable area: 190 mm x 170 mm
Stage positioning resolution: λ/1024 (~0.6 nm)
Beam current stability: 0.2% pp/hr
Beam position stability: ≤60 nm pp/hr (HT) / ≤10 nm pp/hr (HR)
Substrate thickness compatibility: 225 μm to 1.3 mm
Deflection amplitude correction and objective-lens focus correction, using the substrate height detector
Smallest features size: 4.2 nm (demonstrated by JEOL in Development of the JBX-8100FS Electron Beam Lithography System).
The JBX-8100FS is mounted on a TMC Quiet Island with STACIS III antivibration supports. Transmission is minimized at high frequencies, and unlike older anti-vibration supports, is reduced at low (<10 Hz) frequencies as well.
Sample Requirements and Preparation
Samples need to be free of outgassing contaminants, and PR must be properly baked to avoid contamination of the column
Standard Operating Procedure
SOP - JEOL JBX-8100FS E-Beam Writer
Process Control Information
Process Control Context
The JEOL system is calibrated by staff every 7 - 21 days, with separate calibration necessary for each condition file (current). These are typically stable for 1-3 weeks. As part of this process, column shift and tilt is adjusted (similar to an SEM), current is measured (and adjusted via the column zoom lenses, if necessary), wobble is checked and minimized (via the objective aperture, again similar to an SEM), focus and astigmatism is adjusted (via the objective lens strength and stigmator correction values), and the DAILYCAL file is run to ensure everything passes.
Data is shown for the current FEG and previous FEG. These are replaced approximately every 2 years.
Some particularly relevant measurements are shown below:
Current: specified as nominal values. As part of the exposure, the machine will measure the current (by default, every 20 minutes) and automatically adjust the exposure dose based on this. As such, drifts in current will not directly affect the writing quality, but may affect user experience on the system.
How is this set?
Current is a result of the particular characteristics of the emitter at a given point in its lifetime (which may increase or decrease current at the sample), the staff set values of shift and tilt (which should maximize it), and most importantly, the values of the zoom lenses in the column. Current is adjusted by adjusting the zoom lenses. This is not done frequently due to the needed time for accurate adjustment, and the minimal impact on write quality that current drift has for users. Current settings are adjusted whenever a particular condition file is getting close to the specification limit.
How is this measured?
The system moves to the Faraday cup and takes, takes a number of instantaneous measurements of the current, and averages them together.
Upper specification limit: the nominal current itself
Via the dose equation, too high of a staff set current may cause the machine to need a clock speed higher than 125 MHz if a user chooses a typical clock speed very close to the limit (e.g. typically >=120 MHz). This would result in an error message when trying to create the magazine file. From the user standpoint, this could only be remedied by increasing the minimum dose (not usually desirable, as this may overdose your pattern) or increasing the shot pitch (which may or may not result in different pattern results, but is also generally not desirable because of the unknown effect on your results). As a result, staff endeavor to keep the actual current below the nominal current at all times.
Lower specification limit: 10% less than the nominal current
Too low of a current (within reason) will not in anyway harm the pattern, but the write will take longer than expected. If the write is limited by the beam on time, 10% lower current (90% of the specified current) will take ~11% longer to write (100%/90% ≅ 1.11). This is considered a reasonable error, but longer than ~11% may unexpectedly prolong the write, and thus staff will endeavor to keep the actual current not lower than 10% lower than the nominal current.
Calibration measured beam size: The beam size in the X and Y directions measured by the system on a “clean” spot of the AE mark used by staff for calibration. This will always be larger than the true size of the beam, and is only useful in the context explained here.
How is this set?
This is set by having proper alignment by staff of the blanking aperture, shift, tilt, focus, and astigmatism. Additionally, as a particular mark is used to for measurement of the beam size, it will get “contaminated”, artificially inflating the measured beam size. Staff will slightly move the measured position every week, but there is still some low level inflation of the measured beam size that may not be real due to this mark contamination.
How is this measured?
The beam is scanned over a metal knife edge on top of a current detector, which does math to obtain the size of the beam, assuming it is Gaussian. There are scans in both the X and Y direction. The Gaussian assumption is a good assumption at low beam currents (< 30 nA) and an increasingly poorer assumption at high beam currents (> 30 nA), so this value is only given for low currents. Note that the values here will be lower than values given when the focus program is run as part of DAILYCAL because a less clean mark is used for that (which in no way means the beam is actually larger, nor does it negatively affect the write quality). A less pristine mark position is used for writes vs. calibrations because the machine will still properly focus even if the mark is slightly contaminated. The mark positions are moved as needed by staff to ensure a clean enough mark is used at all times.
Upper specification limit: theoretical beam size plus an inherent scattering factor due to the measurement technique plus an allowable blur.
Lower specification limit: none.
Astigmatism:
How is this set?
The focus program is run in a different mode, which measures the beam size at different focus and stigmator values, and find the minimum size across these different values.
How is this measured?
The astigmatism value returned is the number of DAC points between the X and Y best focus values per a curve fit.
Upper specification limit: + 20 DAC points.
Lower specification limit: - 20 DAC points.
High currents (>30 nA) have their focus and astigmatism set manually by staff rather than through the built-in calibration routines on the system. Similarly, the built-in measurement programs do not give reliable values for beam size or astigmatism. As a result, only beam current (which is measured similarly and reliably compared to low currents) is posted here.
Process Control Charts
Process Library
Currently empty, please contribute your processes here.
8100calculator.xlsx
Use this Excel file to assist with picking currents, shot pitches, ensuring you're within the clock headroom (<125 MHz, >8ns), to roughly estimate your write time based on the current/dose/pattern area, and track alignment mark locations.
References
BNC Staff Presentations - Internal Resources
Purdue's JBX-8100FS, from JEOL - Internal Resources
JEOL Manuals - Internal Resources
General References
JEOL
JEOL USA Semiconductor Equipment Documents - Electron Beam Lithography
Georgia Tech
100 kV Electron Beam Lithography System: JBX-9300FS
"JEOL JBX-9300FS Electron Beam Lithography System Training", Georgia Tech
Yale
YINQE EBL - Manuals and Documentation
YINQE EBL - Software Downloads
YINQE EBL - Electron-Beam Lithography Training
University of Washington
Cornell
Shot Pitch and Write Time Calculator - XLS
University of Michigan
University of Minnesota
Vistec EBPG5000 (with good process resources)
Electron Properties
Relevant Literature
"5-nm-Order Electron-Beam Lithography for Nanodevice Fabrication," K. Yamazaki and H. Namatsu, japanese Journal of Applied Physics 43, 3767 (2004).
This paper explains why the measured beam size on the knife edge mark (AE mark) is so much larger than the actual beam size. It further discusses some ultrasmall patterns in HSQ
Partnership Opportunities - Alternate EBL Resists/Processes
Contact Justin Wirth if you are interested in partnering with BNC to evaluate these resists and develop standard processes of broad usefulness to the BNC research community.
AR-P 6200 and AR-N 7520 are of particular interest:
AR-P 6200:
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