Panasonic E620 ICP RIE Etcher

2024-12-20 to 2025-01-02: Reduced Holiday Operations

Dear Birck Research Community,

The Purdue winter recess begins effective Friday afternoon December 20th and concludes Thursday morning, January 2. The university is officially closed during this time. As we have done in past years, the Birck Nanotechnology Center will remain available for research but will be unstaffed and hazardous gasses will be unavailable. Lab work may otherwise proceed, though any fume hood work must be done with someone else present in the same laboratory or cleanroom bay (the "buddy" system). Click the link above to get more detail about equipment conditions and rules.


Refer to the Material and Process Compatibility page for information on materials compatible with this tool.
Equipment Status: Set as UP, PROBLEM, or DOWN, and report the issue date (MM/DD) and a brief description. Italicized fields will be filled in by BNC Staff in response to issues. See Problem Reporting Guide for more info.

StatusUp !
Issue Date and Description


Estimated Fix Date and Comment

The Vacuum issue has been resolved.   With a new pump, and a difficult to reach o-ring replaced, it's working great.

Responding StaffFrancis

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iLab NameC - Panasonic E620 ICP RIE Etcher
iLab KioskBRK Etch Core
FICShared
OwnerFrancis Manfred
LocationCleanroom - K Bay
Max. Wafer6"/150 mm (JEIDA)
Internal Page/wiki/spaces/BNCWiki/pages/6235694

Overview

TypeMaterialsRestricted MaterialsAvailable GasesMax RF PowerWafer Size
ICP RIESi, Oxides, III-IV's, Ti, Al, SiCAu, Ag, Pt, CuO2, Ar, SF6, CHF3, CF4, Cl2, N2, BCl31250 ICP / 600 Platen6 inch (150 mm) JEIDA Specification

General Description

This inductively coupled plasma system etches a wide variety of substrates, including III-V materials, polymers, and metals.

Specifications

The Panasonic E620 is a plasma etch tool capable of using a 1250 watt inductively coupled RF plasma and 600 watt capacitive bias allowing for highly anisotropic etches. It etches a wide range of materials using Ar, CHF3, CF4, SF6, Cl2, N2, O2, and BCl3 as process gasses. Samples are cooled by way of helium backside cooled electrostatic chuck. Additional features include end point monitoring, error logging, and storage for 99 recipes.

Technology Overview 

Gold (Au), Silver (Ag), Copper (Cu), and Platinum (Pt) are NOT allowed in the chamber in any amounts.

Sample Requirements and Preparation

Samples must be mounted to a 150 mm JEIDA standard wafer. Common mounting adhesives are crystalbond and photoresist. "Panasonic wafers" can be purchased from the building supply room during office hours. Gold, silver, copper, and platinum do not have a vapor phase etch byproduct, and are therefore not allowed in the chamber. E-mail the tool engineer for more information on permissible materials.


Standard Operating Procedure                               Recovering Stuck Wafer

                                                                                      

Supplements:

 

Questions & Troubleshooting

 

How do I fix the Panasonic when my wafer gets stuck and I can't unload it in the TEST mode?

This fix applies to when the Panasonic won't run at all.    Please see the attachment named "Recovering Stuck Wafer".

Why won't recipe 103 (Post Chlorine Clean) run?

Check your process gases. That CF4-based recipe won't run if SF6 is enabled. Note that the same protections are not enabled on user-created recipes.

How do I add those protections to my CF4 based recipes?
Copy step 1 from recipe 103 into your recipe. The step flows the gas at 160 sccm. If SF6 is currently selected gas it won't be able to flow, and cause your process to abort before any damage is done.

Is the Panasonic capable of End Point Monitoring (EPM)?
While the tool is equipped with end point detection capabilities, using EPM requires new and specific setup for each different material stack. Additionally, the knowledge of how to setup and operate EPM was lost some time ago. Please contact BNC staff if you are interested in using/learning how to use these capabilities. These documents are available as references: Procedure of EPM setting (Internal Resource), and EPM manual (Internal Resource).

Do I need to adjust the Cooling Helium flow rate or pressure?
Generally the helium flow rate is not important to the etch itself, it is present to monitor a leak in the ESC clamping of the substrate. However, helium pressure has a direct effect on the cooling of the substrate and may need to be adjusted. Pressures from 400 to 1000 Pa are reasonable for most processes.

Do I need to use crystal bond to mount my sample to the carrier wafer?
Crystal bond (or another adhesive, discuss with Sean if you would like to user something else) is necessary both to keep the sample from flying off in the chamber, and to establish good thermal contact between the sample and the carrier wafer. The lack of crystal bond (or another thermal compound) will cause poor and inconsistent cooling for your sample, leading to inconsistent results of the etch process.

What if our Panasonic is down and I need to etch on another, similar system?

UC Santa Barbara has a similar system that may meet remote processing needs for already-developed recipes.

For more information send a message to Tom Reynolds or Brian Thibeault for remote processing.

Process Library

Manufacturer recipes (Internal Resource)

Titanium Etch (Internal Resource)

CF4 Clean (Post Cl etch clean) (Internal Resource). Standard and up-to-date recipe is already on tool, this potentially out of date version is provided here only for reference.

Oxide vertical etch (Internal Resource)

O2 clean (Internal Resource)

Oxide clean and coat (run prior to CHF3 etching) (Internal Resource)

Oxide etch, high selectivity (Internal Resource)

Cl2 clean and coat (before Cl etch) (Internal Resource). Standard and up-to-date recipe is already on tool, this potentially out of date version is provided here only for reference.


Etch material notes:

SiC is very difficult to etch isotropically, and etching of the sidewalls only occurs via heating.

References

Manufacturer References:

Purdue Manufacturer Acceptance Test (Internal Resource)

Manufacturer Website

Manufacturer Manual (Internal Resource)

/wiki/spaces/BNCWiki/pages/6235694

 

Literature References:

Growth of Si-o-Cl polymer during chlorine etching: "Deposition of silicon oxychloride films on chamber walls during Cl2/O2 plasma etching of Si," S. J. Ullal, JVST A 20, p. 499 (2002)

 

External Facilities:

"ICP Etching Recipes," UCSB


ISSUES:


Oct 21, 2021

Some users have not been using the correct procedure when changing gases.   Changing a gas requires 3 steps, and they are summarized below.  Your etch will not turn out correctly unless you follow this procedure.


        Procedure Used When Gases Are Changed

  1.  Move the switch to the appropriate gas on the blue gas selection panel to the left of the machine.
  2. Now the gas line needs to be purged of the previous gas. Select the appropriate Line Purge Recipe and modify it (if necessary) to the conditions shown below:

          

From Old Gas

To      New Gas

Use Recipe #

Time Change  To:

Flow Rate Change  To:

CF4

SF6

107

4:00

170

SF6

CF4

107

5:30

110

CHF3

Ar

106

13:00

50

Ar

CHF3

106

9:00

140

             

          

      3.  Load Recipe 106 or 107 and hit start

      4.  When the recipe is finished, set the correct parameters to the Mass Flow Controller (MFC):

  •  This is found in the “Machine Parameters” menu F11, then “FULL SCALL”  menu F2.
  • You only need to change the Gas name and the FC. (constant fraction) setting for the process gas you plan to use.